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14,15 It involves three steps: the first is the synthesis of 4,4-thiobis(benzenethiol) 8, by chlorosulfonation of diphenylsulfide followed by reduction as outlined in Scheme 4, the second is the nucleophilic condensation polymerization of this dithiol with and 4,4-dichlorodiphenylsulfone 9 under conditions of high dilution; finally, the resulting macrocycles are oxidized to sulfone-linked paracyclophanes.
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